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Thermal analysis, X-ray powder diffraction and electron microscopy data related with the production of 1:1 Caffeine:Glutaric Acid cocrystals
The data presented in this article are related to the production of 1:1 Caffeine:Glutaric Acid cocrystals as part of the research article entitled 鈥淕reen production of cocrystals using a new solvent-free approach by spray congealing鈥 (Duarte et al., 2016)聽[1]. More specifically, here we present the thermal analysis and the X-ray powder diffraction data for pure Glutaric Acid, used as a raw material in聽[1]. We also include the X-ray powder diffraction and electron microscopy data obtained for the 1:1 Caffeine:Glutaric Acid cocrystal (form II) produced using the cooling crystallization method reported in 鈥淥perating Regions in Cooling Cocrystallization of Caffeine and Glutaric Acid in Acetonitrile鈥 (Yu et al., 2010)聽[2]. Lastly, we show the X-ray powder diffraction data obtained for assessing the purity of the 1:1 Caffeine:Glutaric cocrystals produced in聽[1].